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Mono Sodium Phosphate Dihydrate is manufactured by method in which using either phosphate rock or dicalcium phosphate or any similar phosphatic material as a base material from which the mono-sodium phosphate is produced. Phosphate rock, dicalcium’ phosphate, or a similar hosphatic material /is reacted. upon by sulphuric, acid and water sufficient in amount to produce mono-calcium phosphate according to the well-known reaction. After the completion of the above reaction the calcium sulphate is removed by filtration and washed with water until entirely free from mono-calcium phosphate.